Chemical Analysis. Francis Rouessac

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Chemical Analysis - Francis Rouessac


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MEANS OF A SPECTRAL LIBRARY 16.8 ANALYSIS OF THE ELEMENTAL COMPOSITION OF IONS 16.9 FRAGMENTATION OF ORGANIC IONS 16.10 PROTEIN ANALYSIS 16.11 ICP‐MS COUPLING KEY POINTS OF THE CHAPTER PROBLEMS SOLUTIONS

      23  Chapter 17: Isotopic Analyses and Labelling Methods 17.1 PRINCIPLE OF ISOTOPIC DILUTION METHODOLOGIES 17.2 MEASUREMENT BY ADDING A RADIOISOTOPE 17.3 MEASURING BY ADDING A STABLE ISOTOPE 17.4 MEASURING ISOTOPE RATIOS FOR AN ELEMENT 17.5 MEASUREMENTS USING ENZYMATIC LABELLING 17.6 NEUTRON ACTIVATION ANALYSIS (NAA) 17.7 REVIEW OF RADIOACTIVE ISOTOPES 17.8 HALF‐LIFE τ, RADIOACTIVITY CONSTANT λ AND ACTIVITY A 17.9 RADIOACTIVE LABELLING OF ORGANIC MOLECULES 17.10 DETECTION AND COUNTING OF RADIOACTIVITY 17.11 SPECIAL PRECAUTIONS KEY POINTS OF THE CHAPTER PROBLEMS SOLUTIONS

      24  Chapter 18: Specific Analysers 18.1 SPECIFIC ANALYSES 18.2 ELEMENTAL ORGANIC ANALYSIS 18.3 TOTAL NITROGEN ANALYSERS (TN) 18.4 TOTAL SULFUR ANALYSERS 18.5 TOTAL CARBON ANALYSERS (TC, TIC, AND TOC) 18.6 MERCURY ANALYSERS 18.7 ION MOBILITY SPECTROMETRY (IMS) 18.8 KARL FISCHER VOLUMETRIC METHOD KEY POINTS OF THE CHAPTER PROBLEMS SOLUTIONS

      25  Chapter 19: Potentiometric and Ionometric Methods 19.1 MEASUREMENT CELLS 19.2 THE PH ELECTRODE 19.3 ION‐SELECTIVE ELECTRODES (ISE) 19.4 QUANTIFICATIONS METHODS 19.5 APPLICATIONS KEY POINTS OF THE CHAPTER PROBLEMS SOLUTIONS

      26  Chapter 20: Voltammetric Methods 20.1 THE VOLTAMMETRIC METHOD 20.2 THE DROPPING MERCURY ELECTRODE 20.3 DIRECT CURRENT POLAROGRAPHY (DCP) 20.4 DIFFUSION CURRENT 20.5 PULSE POLAROGRAPHY 20.6 ALTERNATING CURRENT POLAROGRAPHY (ACP) 20.7 STRIPPING VOLTAMMETRY 20.8 COULOMETRIC MEASUREMENTS 20.9 COULOMETRIC TITRATION OF WATER CONTENT 20.10 VOLTAMMETRIC DETECTION IN HPLC AND HPCE 20.11 AMPEROMETRIC SENSORS KEY POINTS OF THE CHAPTER PROBLEMS SOLUTIONS

      27  Chapter 21: Sample Preparation 21.1 THE NEED FOR SAMPLE PRETREATMENT 21.2 SOLID PHASE EXTRACTION (SPE) 21.3 IMMUNO‐AFFINITY EXTRACTION 21.4 MICRO‐EXTRACTION PROCESSES 21.5 GAS EXTRACTION ON A CARTRIDGE OR A DISC 21.6 HEADSPACE 21.7 SUPERCRITICAL PHASE EXTRACTION (SPE) 21.8 MICROWAVE REACTORS 21.9 ON‐LINE ANALYSERS KEY POINTS OF THE CHAPTER

      28  Chapter 22: Basic Statistical Parameters 22.1 CENTRAL VALUE, ACCURACY, AND RELIABILITY OF A SET OF MEASUREMENTS 22.2 VARIANCE AND STANDARD DEVIATION 22.3 RANDOM OR INDETERMINATE ERRORS 22.4 CONFIDENCE INTERVAL


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